Electrolysis is the least commonly used method in the synthesis of carbon nanotubes. In this method, two graphite electrodes are immersed in molten ionic salts and current is passed through. After completion of the electrolysis process, the remaining carbonaceous material is dissolved in distilled water. This dissolves the ionic salt, and the dispersion is separated by filtration. The residues contain a mixture of carbon filaments, amorphous carbon, remnants of the salt ions, which cove some of the carbon, and multi-walled carbon nanotubes. However, the electrolysis method cannot be used in the production of single-walled carbon nanotubes.
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